I'm late to the party on this topic, but it might be useful for anyone else treading down this path.
I'm using a Microtech PCD-25BH on an A4000 with GVP-TREX-II SCSI-II. Presently, it is working reliably. I did have some similar issues with random errors. After switching to Microtech branded PCMCIA-CF adapters, problems went away.
Other potential problems were mentioned in previous posts. CF cards vary, if one brand doesn't work, try another. No name cheap cards may be more trouble.
SCSI cabling and proper termination may be another fault. I believe termination is at the root of my current issue. I only have this microtech drive on the GVP SCSI and want to add a second drive, but none are being seen. I likely need to remove or disable termination on the microtech drive.
On termination, you may need to use active vs passive, depending on your controller. If you are using any adapters, like 50pin to 68pin, you may also need one terminates the unused pins.
It's also worthwhile to clean your connectors with something like deox-it.
FYI, one document I found suggests that the microtech drive is rated for 4MB/sec transfers. I have not speed tested this myself though. ZuluSCSI Blaster is faster.
Jaeson